Re: Supplements exposed
Good info thanks. The Det. Temp and Det.HV are shown real time on the bottom right hand corner of the DPPMCA program- good idea to moniotor those for stability or changes. Should be stable over many
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GEOelectronics@...
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#1493
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Re: Supplements exposed
GeoThis is from Amptek troubleshooting guide?
If the resolution is worse than you expect, then ...Check for good coolingIn Amptek¡¯s thermoelectrically cooled detectors, the back of the detector is
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taray singh <sukhjez@...>
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#1492
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Re: Supplements exposed
" Tip for calibration
It can be difficult to find 2 peaks at extreme end within a specimen or combination.
Sometimes with this method it is difficult to identify peaks
Easier way is use 2 different
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GEOelectronics@...
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#1491
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Re: Supplements exposed
Here is pic of selenium sulphide(dried centrifugal sample of selenium sulphide suspension / Selsun) using 2048 with threshold correction.
The selenium peaks are seen clearly? and not hidden like the
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taray singh <sukhjez@...>
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#1490
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Re: Si pin xrf ..1st go
Geo,
These ¡°peaks¡± look to be counting noise. The difference between Kb1 and Kb2 is just 0.013 while the peak difference is 0.08 keV
Dud
Sent: Saturday, October 24, 2020 6:15 AM
To:
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Dude
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#1489
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Re: Trinitite
There is quite a big mass difference between a piece of DU and the little amount Pu decay in the Trinitite. There can also be a big difference in detector efficiencies.
Dud
Sent: Friday, October 23,
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Dude
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#1488
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Re: Si pin xrf ..1st go
Again no problem. Lowering your max energy to 62 like I do will give more precisi8on per channel. Nothing above 60 will register normally anyway.
Just keep it high enough to see 59.5 for calibration
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GEOelectronics@...
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#1487
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Re: Si pin xrf ..1st go
Made a Math mistakeIt¡¯s 0.04 not 4At least now I know the relevance of this channel settings?I was taken off guard?I actually did a SF threshold check after calibration?But ?din register when I
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taray singh <sukhjez@...>
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#1486
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Re: Si pin xrf ..1st go
Taray,
With the 2048 conversion gain your max energy is 88.76 keV so one channel is 88.76/2048 = 0.043 keV/channel. See if one right or left arrow click will give you a 0.04 energy difference.
Dud
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Dude
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#1485
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Re: Si pin xrf ..1st go
Very interesting set up thanks for sharing.
You need to get rid of the low energy noise as your dead time is 100% with over 10 million noise counts. Run the fast and slow thresholds ad check your
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Dude
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#1484
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Re: Si pin xrf ..1st go
Taray,
Set cursor somewhere in middle of scan.
Move 1 click left, then 1 click right of original spot. Record keV readings.
Temporarily click off CAL (ICON #18) , repeat test. Record channel #'s
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GEOelectronics@...
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#1483
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Re: Si pin xrf ..1st go
Taray- show me in pictures offlist or onlist OK?Geo
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GEOelectronics@...
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#1482
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Re: Si pin xrf ..1st go
Charles,
In the chart below, ignore the intensity%- it has no meaning in this context, but the X-Ray transition energies do.
.
Check out the different K lines on the chart, what you are seeing as
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GEOelectronics@...
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#1481
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Re: Si pin xrf ..1st go
Anyone knows how to control the energy cursor.Each I move the rt left pc keyboard,it moves by 4 units,Abit too much ?for peaks.Centroid ?method?is ?an?alternative but not?so easyTaray
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taray singh <sukhjez@...>
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#1480
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Re: Si pin xrf ..1st go
CharlesJust noticed thatNee?fast?threshold was 16Did not save it b4 posting?
Taray
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taray singh <sukhjez@...>
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#1479
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Re: Si pin xrf ..1st go
Using a convex mount for your buttons is very interesting. I may have to
try that.
Is your input rate always so high? Mine is typically in the 10 to 20
range. Have you done the Tune Slow/Fast
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Charles David Young
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#1478
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Re: Si pin xrf ..1st go
Taray,
Thanks for the post.? I am in the process of coming up with a similar Am241 device.? It is great that you found that Nickel line with your meteorite, that is useful information also.
Mike
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Mike L.
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#1477
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Re: Si pin xrf ..1st go
Dud
remarkably efficient source / geometry set up...
I am not sure but maybe this is why.?I am using a slightly convex ludlum collimator lead disc
? 9 Am241 exciter are glued on? the outer edge?
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taray singh <sukhjez@...>
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#1476
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Re: Trinitite
Many Pu isotopes lead to uranium, but if one of the precursors is half-life in the millions of years, there won't be very many atoms of U being made now from those in our sample from 1945. If
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GEOelectronics@...
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#1475
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Re: Trinitite
Of course I agree. But given the very accurate ICP-mass spectrometer analysis of this material made by national labs, not by a youtuber, what known isotopes would cause these particular 3 X-Ray
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GEOelectronics@...
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#1474
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