A PerkinElmer Elan 6000 - that thing must weigh a ton!? Which Shimadzu unit do you have? Is this for a home lab!?? If so that it is awesome. I hope you're not using H2 for carrier gas lol.??
Sephadex G-25 for affinity chromatography I assume?? G-10 is for small molecule.? I guess it depends on what you're interested in.? Are you looking for more residual solvents? Or understanding more about the dye and/or additional additives?
GC would require a midpolar column.? Something like Agilent's VF-35ms.? Good for resolving aromatics with substituted?polar groups.? Still think it is unlikely you'd be able to find a method that would resolve all components of the dye on GC-MS considering the molar mass of the dye.
On Fri, Oct 4, 2024 at 9:15?PM gren via <hrgerson=[email protected]> wrote:
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Don't think I need an outside lab, .... but would be interested in discuss with those actually having analytical equipment.
(? I still need a few minor parts for my pe Elan 6000,? so that is not ready yet,? lol.? And yes, I would need a different column for the Shimadzu, sigh. )
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But, am betting that this ink issue can be solved more easily:
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My next practical step, after having tried some TLC plates, will be to try one of the inexpensive Sephadex columns,
Will start with either G-10 or G-25, and then possibly proceed forward, with a more specific column.