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Ken's "Mystery Wire"


 

Member Ken S sent in a wire labeled "Mystery Wire".

It is silver in color, very hard but not springy. Non magnetic. Extremely light for its volume.
Many more tests to be done, but XRF was easy, and based on the elemental makeup my best guess as of today is one of the super alloys under ASTM B649-17


ASTM B649 - 17

Standard Specification for Ni-Fe-Cr-Mo-Cu-N Low-Carbon Alloys (UNS N08925, UNS N08031, UNS N08034, UNS N08354

Small mass, non magnetic even though Fe is major, low Ni content, low Cu content. Not a Nicrome, maybe an Alchrome?


Mystery-Wire-53kVp-20uA-180s-Notes-pic.png

Will test further, hardness, electrical resistivity, thermal conductivity,? radioactivity etc.

Geo


 

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Thanks for scanning the wire, Geo.? Interesting results, though not surprising.? Although a magnet won’t pick it up, not even a good neodymium magnet, a tiny neodymium magnet will “stick” to it, indicating that it is slightly magnetic.? As you’ve ascertained, it is very hard, to the point it is difficult to cut it with wire cutters.? Well, at least, much more difficult than similar gauge iron or steel wire.

?

I pulled out a cheap micrometer (0.05 mm resolution), and the diameter comes out somewhere between 0.95 and 1.00 mm, or roughly 18-gauge.? Assuming a diameter of 0.975 mm, or 0.0975 cm, the cross-sectional area is 7.47E-3 cm^2.? A 10-cm piece of the wire would have a volume of 0.0747 cm^3, and has a mass of 0.65 grams.? That would equate to a density of 8.7 g/cm^3.? For comparison, here’s a table of the densities of the various elements that showed up in Geo’s XRF scan:

Cr:? 7.19 g/cm^3

Fe:? 7.88 g/cm^3

Ni:? 8.90 g/cm^3

Cu:? 8.92 g/cm^3

Mo: 10.22 g/cm^3

Ru: 12.41 g/cm^3

Sn:? 7.29 g/cm^3

?

It is moderately resistive as well, though nowhere as resistive as nichrome.? Many years ago I made up a jig consisting of a regulated DC voltage source feeding a chain of a 3-ft chunk of the wire in series with a 1% 100-ohm resistor.? I had a digital multimeter in the chain measuring the total current flowing through the series circuit, and then used another digital multimeter to measure the voltage across each of the individual ‘resistors’ in the circuit.? It was easy enough to use Ohm’s Law to solve for the “unknown” resistance represented by the 3-ft length of “mystery wire”…? R = E ÷ I.? I don’t remember the results now, but perhaps I’ll try to cobble the setup together again and repeat the experiment.? If I get the chance, I’ll report the results here.

?

Thanks again, George.

?

Ken, WB?OCV?

East Falmouth, MA USA

?

?

From: GEOelectronics@...
Sent: Wednesday, January 29, 2020 01:17 PM
To: [email protected]
Subject: [XRF] Ken's "Mystery Wire"

?

Member Ken S sent in a wire labeled "Mystery Wire".

It is silver in color, very hard but not springy. Non magnetic. Extremely light for its volume.
Many more tests to be done, but XRF was easy, and based on the elemental makeup my best guess as of today is one of the super alloys under ASTM B649-17


ASTM B649 - 17

Standard Specification for Ni-Fe-Cr-Mo-Cu-N Low-Carbon Alloys (UNS N08925, UNS N08031, UNS N08034, UNS N08354

Small mass, non magnetic even though Fe is major, low Ni content, low Cu content. Not a Nicrome, maybe an Alchrome?
Will test further, hardness, electrical resistivity, thermal conductivity,? radioactivity etc.

Geo

_._,_._,_

?


 

"Interesting results, though not surprising.? Although a magnet won’t pick it up, not even a good neodymium magnet, a tiny neodymium magnet will “stick” to it, indicating that it is slightly magnetic."

Good tip and I'll try to remember to add that to my bag of tricks. What you describe might be "paramagnetic", the ability of an atom to display weak magnetism but only in the presence of a strong magnetic field. Titanium is one metal known for that, so is aluminum. Fe (iron) is of course a ferromagnetic atom, but when combined with another atom, becomes paramagnetic. molecule, for example FeO.

Please do try to look up your resistance readings, we can compare them to my results.

Aluminum is difficult to XRF in the amateur lab. But perhaps the magnetic susceptibility meter will give us a number.

Also the Mohs scratch test will give us a hardness, at least to the nearest whole number.

Supermetals are a hoot.

Geo



----- Original Message -----
From: Ken Sejkora <kjsejkora@...>
To: [email protected]
Sent: Thu, 30 Jan 2020 07:42:20 -0500 (EST)
Subject: Re: [XRF] Ken's "Mystery Wire"

Thanks for scanning the wire, Geo.? Interesting results, though not surprising.? Although a magnet won’t pick it up, not even a good neodymium magnet, a tiny neodymium magnet will “stick” to it, indicating that it is slightly magnetic.? As you’ve ascertained, it is very hard, to the point it is difficult to cut it with wire cutters.? Well, at least, much more difficult than similar gauge iron or steel wire.

?

I pulled out a cheap micrometer (0.05 mm resolution), and the diameter comes out somewhere between 0.95 and 1.00 mm, or roughly 18-gauge.? Assuming a diameter of 0.975 mm, or 0.0975 cm, the cross-sectional area is 7.47E-3 cm^2.? A 10-cm piece of the wire would have a volume of 0.0747 cm^3, and has a mass of 0.65 grams.? That would equate to a density of 8.7 g/cm^3.? For comparison, here’s a table of the densities of the various elements that showed up in Geo’s XRF scan:

Cr:? 7.19 g/cm^3

Fe:? 7.88 g/cm^3

Ni:? 8.90 g/cm^3

Cu:? 8.92 g/cm^3

Mo: 10.22 g/cm^3

Ru: 12.41 g/cm^3

Sn:? 7.29 g/cm^3

?

It is moderately resistive as well, though nowhere as resistive as nichrome.? Many years ago I made up a jig consisting of a regulated DC voltage source feeding a chain of a 3-ft chunk of the wire in series with a 1% 100-ohm resistor.? I had a digital multimeter in the chain measuring the total current flowing through the series circuit, and then used another digital multimeter to measure the voltage across each of the individual ‘resistors’ in the circuit.? It was easy enough to use Ohm’s Law to solve for the “unknown” resistance represented by the 3-ft length of “mystery wire”…? R = E ÷ I.? I don’t remember the results now, but perhaps I’ll try to cobble the setup together again and repeat the experiment.? If I get the chance, I’ll report the results here.

?

Thanks again, George.

?

Ken, WB?OCV?

East Falmouth, MA USA

?

?

From: GEOelectronics@...
Sent: Wednesday, January 29, 2020 01:17 PM
To: [email protected]
Subject: [XRF] Ken's "Mystery Wire"

?

Member Ken S sent in a wire labeled "Mystery Wire".

It is silver in color, very hard but not springy. Non magnetic. Extremely light for its volume.
Many more tests to be done, but XRF was easy, and based on the elemental makeup my best guess as of today is one of the super alloys under ASTM B649-17


ASTM B649 - 17

Standard Specification for Ni-Fe-Cr-Mo-Cu-N Low-Carbon Alloys (UNS N08925, UNS N08031, UNS N08034, UNS N08354

Small mass, non magnetic even though Fe is major, low Ni content, low Cu content. Not a Nicrome, maybe an Alchrome?
Will test further, hardness, electrical resistivity, thermal conductivity,? radioactivity etc.

Geo





 

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Hi Geo,

?

I moved in June 2019, so there are still boxes of junk (er, I mean “components”) waiting to be unpacked.? I couldn’t find my 1% 100-Ohm power resistor or original test jig, but was able to dig up a 3% 110-Ohm 25-watt resistor and some jumper wires.? I found the longest piece of the mystery wire I could easily lay out on the floor to measure, and it came out to 354 inches, or just shy of 900 cm.? Hooked up in series with the 110-Ohm resistor to a 12-volt regulated power supply, the average current through the circuit was 100.5 mA, producing a voltage of 807.3 mV across the mystery-wire resistor.? Solving by Ohm’s law, the resistance worked out to 807.3 mV ÷ 100.5 mA = 8.033 Ohms.? Dividing by the length of wire (899 cm), that works out to a resistivity of 0.00893 Ohms/cm.? Converting to more conventional units, that’s 893 Ohms/1000 meters, or 272 Ohms/1000 ft.? By comparison, 18-gauge copper wire (closest to 0.975 mm dia), has a resistivity of 20.94 Ohms/1000 meters.? Bottom line, the “mystery wire” has a resistivity that is 43-times greater than that of similar-sized coper wire.? I tried a shorter length of wire, as well as different power supply voltages, and all of the resistivity measurements came out very close to 0.0089 Ohms/cm.

?

For what it’s worth, the power dissipation through the 110-Ohm resistor was about 1.1 Watts, and about 0.08 Watts through the 900-cm length of wire.? With these low power dissipation values, there should have been minimal heating effects that could affect the resistance as the components heated up.

?

I hope this helps? --? Ken

?

From: GEOelectronics@...
Sent: Thursday, January 30, 2020 10:14 AM
To: [email protected]
Subject: Re: [XRF] Ken's "Mystery Wire"

?

Please do try to look up your resistance readings, we can compare them to my results.

?

Geo

?


 

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Greetings to the group,

?

Some more interesting properties of the “mystery wire”.? Although I don’t have a way to quantify the results, I can at least qualify the results.

?

Regarding the magnetic properties of the wire, it appears to be somewhat “neutral”.? I tried to qualify this in two manners.? I hooked up a small solenoid coil to an inductance meter and determined the inductance of the “bare” core,? that is, nothing within the cavity of the core.? The result was 0.42 mH.? As expected, if I introduced a steel screwdriver into the cavity (ferromagnetic composition, that is, can be formed into a ‘permanent’ magnet), the inductance increased (1.53 mH).? If I introduced a few strands of 16-gauge copper wire (diamagnetic composition, that is, repelled by a magnetic field) into the core, the inductance decreased (0.38 mH). ?A roll of aluminum (paramagnetic composition, that is attracted to a magnetic field) also decreased the inductance (0.39 mH).? When I introduced several strands of the mystery wire into the cavity, the inductance didn’t change at all, suggesting that it may be only paramagnetic (attracted to a magnetic field, although in this case only slightly to a strong neodymium magnet).

?

Along a similar vein, I pulled out a cheap metal detector and checked its response to various metals.? When the discriminator was properly tuned and producing a steady tone, a pair of pliers or screwdriver (both steel/iron) produced a softer or absent tone, whereas a spool of copper produced a stronger/louder tone. A spool if the “mystery wire” resulted in no change in the tone when the metal detector passed over it.

?

Although metal, the “mystery wire” appears to be almost ‘neutral’ in its response to a magnetic fields.? Granted, a small piece (<1 cm) of the wire will “stick” very loosely to a strong neodymium magnet, it does not appear to produce any detectable response to my two electromagnetic tests. I will admit neither test is by no means quantitative, but I do find the qualitative results intriguing.

?

When Geo suggested the wire might be some type of “supermetal”, it made me start thinking.? I began to wonder if the composition of the wire was deliberately “tuned” to have a neutral response.? A bit of background into the wire.? I used to work at a facility that had some E-field sensors around it to detect potential intruders.? The “mystery wire” used to be stretched along the perimeter of the facility to detect any objects entering within the vicinity of the wires.? I have no idea if the process worked on detecting changes in inductance, capacitance, or both, but if one were attempting to minimize the inductive response, it might make sense to “tune” the wire composition to be relatively ‘neutral’, that is, neither ferromagnetic (e.g., steel wire), diamagnetic (e.g., copper wire), and minimally paramagnetic.? On top of that, the mixture is strong, stiff, hard, resilient, and has a high tensile strength.? All of these properties would lend well to creating an E-field sensor.

?

All speculation on my part.? Thanks for your analyses, George.? Like you said, aren’t supermetals a hoot??

?

Ken


 

All good tests and yes they add to the knowledge base. Use what you have, make the most of it.

Your last clue was the give away, it's a "taught-wire PID". We won't talk about its tech but we can sure analyze this wire...


Geo

----- Original Message -----
From: Ken Sejkora <kjsejkora@...>
To: [email protected]
Sent: Thu, 30 Jan 2020 17:05:35 -0500 (EST)
Subject: Re: [XRF] Ken's "Mystery Wire"

Greetings to the group,

?

Some more interesting properties of the “mystery wire”.? Although I don’t have a way to quantify the results, I can at least qualify the results.

?

Regarding the magnetic properties of the wire, it appears to be somewhat “neutral”.? I tried to qualify this in two manners.? I hooked up a small solenoid coil to an inductance meter and determined the inductance of the “bare” core,? that is, nothing within the cavity of the core.? The result was 0.42 mH.? As expected, if I introduced a steel screwdriver into the cavity (ferromagnetic composition, that is, can be formed into a ‘permanent’ magnet), the inductance increased (1.53 mH).? If I introduced a few strands of 16-gauge copper wire (diamagnetic composition, that is, repelled by a magnetic field) into the core, the inductance decreased (0.38 mH). ?A roll of aluminum (paramagnetic composition, that is attracted to a magnetic field) also decreased the inductance (0.39 mH).? When I introduced several strands of the mystery wire into the cavity, the inductance didn’t change at all, suggesting that it may be only paramagnetic (attracted to a magnetic field, although in this case only slightly to a strong neodymium magnet).

?

Along a similar vein, I pulled out a cheap metal detector and checked its response to various metals.? When the discriminator was properly tuned and producing a steady tone, a pair of pliers or screwdriver (both steel/iron) produced a softer or absent tone, whereas a spool of copper produced a stronger/louder tone. A spool if the “mystery wire” resulted in no change in the tone when the metal detector passed over it.

?

Although metal, the “mystery wire” appears to be almost ‘neutral’ in its response to a magnetic fields.? Granted, a small piece (<1 cm) of the wire will “stick” very loosely to a strong neodymium magnet, it does not appear to produce any detectable response to my two electromagnetic tests. I will admit neither test is by no means quantitative, but I do find the qualitative results intriguing.

?

When Geo suggested the wire might be some type of “supermetal”, it made me start thinking.? I began to wonder if the composition of the wire was deliberately “tuned” to have a neutral response.? A bit of background into the wire.? I used to work at a facility that had some E-field sensors around it to detect potential intruders.? The “mystery wire” used to be stretched along the perimeter of the facility to detect any objects entering within the vicinity of the wires.? I have no idea if the process worked on detecting changes in inductance, capacitance, or both, but if one were attempting to minimize the inductive response, it might make sense to “tune” the wire composition to be relatively ‘neutral’, that is, neither ferromagnetic (e.g., steel wire), diamagnetic (e.g., copper wire), and minimally paramagnetic.? On top of that, the mixture is strong, stiff, hard, resilient, and has a high tensile strength.? All of these properties would lend well to creating an E-field sensor.

?

All speculation on my part.? Thanks for your analyses, George.? Like you said, aren’t supermetals a hoot??

?

Ken





 

On Thu, Jan 30, 2020 at 04:05 PM, Ken Sejkora wrote:
it might make sense to “tune” the wire composition to be relatively ‘neutral’, that is, neither ferromagnetic (e.g., steel wire), diamagnetic (e.g., copper wire), and minimally paramagnetic.
Interesting. Now that you reminded, I think there are still some neutral coil adjusting tools down in the workshop, left over from the radio says. I'll dig one of those out and test it on XRF. for fun.

If you still have your supermagnet, handy check the ends of the wire vs the sides of the wire with it. There seems to be a dramatic difference. See the video clip:



does that seem normal?

Geo


 

On Thu, Jan 30, 2020 at 01:38 PM, Ken Sejkora wrote:
that works out to a resistivity of 0.00893 Ohms/cm.?
Looks good Ken.?
I get? 0.00850 but the millivoltmeter hasn't been turned on for a while. Will check again tomorrow after leaving it on overnight. One desk in the shop is setup just for resistor testing, we use hand selected resistors in projects and want to be able to test them under actual HV conditions same goes for capacitors.

Geo

Geo


 

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Interesting observation, Geo.? I had noticed the same thing, that the end seems to be more ‘magnetic’ than the sides.? It might be interesting to take a weak magnet and try the same thing with a more strongly magnetic object like a paperclip or small screw.? I’m guessing this phenomenon is NOT unique to the “mystery wire”.

?

I know if you “pick up” a pile of pins or paperclips with a magnet, they stick together end-to-end, versus side-to-side.? Same goes for picking up a screw with a slightly magnetized screwdriver… the attraction seems stronger at the ends of the screw, rather than along its length.? I wonder if the intensity of the magnetic flux is stronger on the small cross section of the end of a relatively long (much larger in length compared to diameter), than if the field is dispersed along the length of the object when picking it up along its side.

?

I’m guessing your observation has more to do with the physics behind magnetic fields, than it has to do with the homogeneity of the elemental composition of the wire itself.? I guess that there might be a possibility the “mystery wire” has an iron/steel core, and is otherwise plated/clad/coated with the other metallic components.? I guess one could stick the wire into the chuck of a drill and grind off the outer layer, and reanalyze it with the XRF.? If there is a coating on the wire, the new XRF should be different than the first.? However, if the wire is homogeneous in composition throughout, then the two spectra should be relatively the same.

?

That was actually the impetus behind my first question related to ‘resolution’ (for lack of better terms) of XRF in delineating a homogeneous-composition alloy from a plated/coated object containing the same elemental mix.? The example of brass alloy versus the copper-clad penny.

?

Thanks for all of your efforts in this inquiry, Geo.

?

I hope everyone has a fantastic weekend --? Ken

?

From: GEOelectronics@...
Sent: Friday, January 31, 2020 04:44 PM
To: [email protected]
Subject: Re: [XRF] Ken's "Mystery Wire"

?

On Thu, Jan 30, 2020 at 04:05 PM, Ken Sejkora wrote:

If you still have your supermagnet, handy check the ends of the wire vs the sides of the wire with it. There seems to be a dramatic difference. See the video clip:



does that seem normal?

Geo

?


 

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Geo,

I don’t have the .mca file but looking at the mystery wire .png the Ka1 Ru reported at 19.7 would actually be the Mo Kb1 at 19.6.

The no match at 15.55 would appear to be a Ni -Cu sum peak at 15.6. ?It’s not real likely you’re actually seeing intrinsic or atmospheric Kr so my best guess would be a Ni-Cr sum peak at 12.8.

If this is from a taught wire PID then we could ?expect it was designed for a very low coefficient of thermal expansion, now how? to test that?

Interesting stuff.

Dud KK7IF

?

?

From: [email protected] [mailto:[email protected]] On Behalf Of GEOelectronics@...
Sent: Wednesday, January 29, 2020 10:12 AM
To: [email protected]
Subject: [XRF] Ken's "Mystery Wire"

?

Member Ken S sent in a wire labeled "Mystery Wire".

It is silver in color, very hard but not springy. Non magnetic. Extremely light for its volume.
Many more tests to be done, but XRF was easy, and based on the elemental makeup my best guess as of today is one of the super alloys under ASTM B649-17


ASTM B649 - 17

Standard Specification for Ni-Fe-Cr-Mo-Cu-N Low-Carbon Alloys (UNS N08925, UNS N08031, UNS N08034, UNS N08354

Small mass, non magnetic even though Fe is major, low Ni content, low Cu content. Not a Nicrome, maybe an Alchrome?


Mystery-Wire-53kVp-20uA-180s-Notes-pic.png

Will test further, hardness, electrical resistivity, thermal conductivity,? radioactivity etc.

Geo


 

开云体育

I think you’re right, Dud.? I questioned the identification of Kr and Ru, but didn’t pursue the possibilities of Kb or sum peaks. Both of your arguments seem like probable explanations given the other constituents in the wire. Krypton would be very unlikely, given its atmospheric content of only 0.000114%. Given that most of the elements in the mystery wire are near-ferrous, the Kb energy from Mo makes more sense for the 19.6 keV peak.

?

Thanks for your insights? --? Ken

?

From: Dude
Sent: Saturday, February 1, 2020 03:48 PM
To: [email protected]
Subject: Re: [XRF] Ken's "Mystery Wire"

?

Geo,

I don’t have the .mca file but looking at the mystery wire .png the Ka1 Ru reported at 19.7 would actually be the Mo Kb1 at 19.6.

The no match at 15.55 would appear to be a Ni -Cu sum peak at 15.6. ?It’s not real likely you’re actually seeing intrinsic or atmospheric Kr so my best guess would be a Ni-Cr sum peak at 12.8.

If this is from a taught wire PID then we could ?expect it was designed for a very low coefficient of thermal expansion, now how? to test that?

Interesting stuff.

Dud KK7IF

?

?

?


 

Here's the one from just now, done with the new filter stack:

Mystery-Wire-XRF-W-New-Filter-Stack-small.jpg

.mca attached.


 

Right now the chamber has a 1" thick aluminum lid, topped with several thin lead "blankets", a flexible shielding material. No leakage out of the top but more importantly no Pb XRF from the old lid shows up in the scan. From this I can design a new lid.

Tweaking the kV and uA, for the mystery wire, concentrating on a starting point,?
we can now ID low Ni/ Chrome Moly Steel in 20 seconds. Next week?
I will start the hunt for some know SS alloy samples at the local steel yard.?
Bottom line, comparing to a known source is always best and easiest, not that they are likely to have any of this particular material on hand.

Ken do you have a 1 gram piece for Dudley?

Folks, would we call this Chrome-Moly Steel, with alloy to be determined later?


Geo
20s-Scan-Chrome-Moly-Steel-.png


 

开云体育

Geo,

My system cal uses a 316 SS disk. Take the wire with you and see if they have a xrf metal analyzer and get an ID that way.

Dud

?

From: [email protected] [mailto:[email protected]] On Behalf Of GEOelectronics@...
Sent: Sunday, February 2, 2020 8:15 AM
To: [email protected]
Subject: Re: [XRF] Ken's "Mystery Wire"

?

Right now the chamber has a 1" thick aluminum lid, topped with several thin lead "blankets", a flexible shielding material. No leakage out of the top but more importantly no Pb XRF from the old lid shows up in the scan. From this I can design a new lid.

Tweaking the kV and uA, for the mystery wire, concentrating on a starting point,?
we can now ID low Ni/ Chrome Moly Steel in 20 seconds. Next week?
I will start the hunt for some know SS alloy samples at the local steel yard.?
Bottom line, comparing to a known source is always best and easiest, not that they are likely to have any of this particular material on hand.

Ken do you have a 1 gram piece for Dudley?

Folks, would we call this Chrome-Moly Steel, with alloy to be determined later?


Geo
20s-Scan-Chrome-Moly-Steel-.png


 

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Geo,

Attached is a manually selected ROI showing the Cr, Fe, Mo, and the missing Ni. ?Using auto generated ROI computer picks usually are not very helpful and in the end its probably best to set your own using a quasi-heuristic approach (by eye-ball) for the ROI’s.

Note that these peaks are noisy and under sampled with the largest peak, Fe, having only 212 counts in it for a 20 sec count.? The count rate is 2306 cps which is slow for this detector which can handle a much higher count rate. ?For your 4.8 usec peaking time you should be able get up to 50,000 cps.? To do that try a couple of things, ?get the detector closer to the target, increase the beam current and optimize the collimator’s beam diameter. ?I suspect? the large standoff distance of the detector may be the most sensitive to the problem.?

The Cal Check.bmp ?attachment is a 30 sec 50 kV shot of a 316 SS calibration disk resulting in a count rate of 31,861 cps.? Note the Fe peak is well defined and has a 1909 count peak.

Dud

KK7IF

?

?

From: [email protected] [mailto:[email protected]] On Behalf Of GEOelectronics@...
Sent: Sunday, February 2, 2020 8:15 AM
To: [email protected]
Subject: Re: [XRF] Ken's "Mystery Wire"

?

Right now the chamber has a 1" thick aluminum lid, topped with several thin lead "blankets", a flexible shielding material. No leakage out of the top but more importantly no Pb XRF from the old lid shows up in the scan. From this I can design a new lid.

Tweaking the kV and uA, for the mystery wire, concentrating on a starting point,?
we can now ID low Ni/ Chrome Moly Steel in 20 seconds. Next week?
I will start the hunt for some know SS alloy samples at the local steel yard.?
Bottom line, comparing to a known source is always best and easiest, not that they are likely to have any of this particular material on hand.

Ken do you have a 1 gram piece for Dudley?

Folks, would we call this Chrome-Moly Steel, with alloy to be determined later?


Geo
20s-Scan-Chrome-Moly-Steel-.png


 

sounds like a great plan, but they count the seconds on their X-Ray tube and won't do any favors......Unless maybe I say I have 500 pounds of "this material" what is it worth?

----- Original Message -----
From: Dude <dfemer@...>
To: [email protected]
Sent: Sun, 02 Feb 2020 14:20:13 -0500 (EST)
Subject: Re: [XRF] Ken's "Mystery Wire"

Geo,

My system cal uses a 316 SS disk. Take the wire with you and see if
they have a xrf metal analyzer and get an ID that way.

Dud

?

From: [email protected]
[mailto:[email protected]] On Behalf Of GEOelectronics@...
Sent: Sunday, February 2, 2020 8:15 AM
To: [email protected]
Subject: Re: [XRF] Ken's "Mystery Wire"

?

Right now the chamber has a 1" thick aluminum lid,
topped with several thin lead "blankets", a flexible shielding
material. No leakage out of the top but more importantly no Pb XRF from the old
lid shows up in the scan. From this I can design a new lid.


Tweaking the kV and uA, for the mystery wire, concentrating on a starting
point,?

we can now ID low Ni/ Chrome Moly Steel in 20 seconds. Next week?

I will start the hunt for some know SS alloy samples at the local steel
yard.?

Bottom line, comparing to a known source is always best and easiest, not that
they are likely to have any of this particular material on hand.


Ken do you have a 1 gram piece for Dudley?


Folks, would we call this Chrome-Moly Steel, with alloy to be determined later?



Geo







 

Here's the 600s scan after doing the work on the beam and lid.Take a good look at Te and Ru lines, can those be real?

600s-Scan-Chrome-Moly-Steel-.jpg


 

Very nice bit of detective work,
Congratulations, Geo.

Randall

----- Original Message -----
From: GEOelectronics@...
To: [email protected]
Sent: Sun, 02 Feb 2020 08:15:07 -0800 (PST)
Subject: Re: [XRF] Ken's "Mystery Wire"

Right now the chamber has a 1" thick aluminum lid, topped with several thin lead "blankets", a flexible shielding material. No leakage out of the top but more importantly no Pb XRF from the old lid shows up in the scan. From this I can design a new lid.

Tweaking the kV and uA, for the mystery wire, concentrating on a starting point,
we can now ID low Ni/ Chrome Moly Steel in 20 seconds. Next week
I will start the hunt for some know SS alloy samples at the local steel yard.
Bottom line, comparing to a known source is always best and easiest, not that they are likely to have any of this particular material on hand.

Ken do you have a 1 gram piece for Dudley?

Folks, would we call this Chrome-Moly Steel, with alloy to be determined later?

Geo


 

Thanks Randall! This is great fun and it's nice to be able to watch the peaks build real-time. It seems the best thing is to do is take a reading at 60 seconds, 300 seconds and 600 seconds for the record, saving each for futu re reference.

Today all of my moly samples (stamps I call them they are the size of a letter stamp) -were tested, holy cow the sheet metal ones are really loaded with minor amendments and contamination not visible on NaI(Tl) (great for moly peaks for cal tho, even on Si-PIN). Also testing the Ni-Mo alloys, pretty interesting.

George

----- Original Message -----
From: Randall Buck <rbuck@...>
To: [email protected]
Cc: [email protected]
Sent: Mon, 03 Feb 2020 13:37:22 -0500 (EST)
Subject: Re: [XRF] Ken's "Mystery Wire"


Very nice bit of detective work,
Congratulations, Geo.

Randall



----- Original Message -----
From: GEOelectronics@...
To: [email protected]
Sent: Sun, 02 Feb 2020 08:15:07 -0800 (PST)
Subject: Re: [XRF] Ken's "Mystery Wire"

Right now the chamber has a 1" thick aluminum lid, topped with several thin lead "blankets", a flexible shielding material. No leakage out of the top but more importantly no Pb XRF from the old lid shows up in the scan. From this I can design a new lid.

Tweaking the kV and uA, for the mystery wire, concentrating on a starting point,
we can now ID low Ni/ Chrome Moly Steel in 20 seconds. Next week
I will start the hunt for some know SS alloy samples at the local steel yard.
Bottom line, comparing to a known source is always best and easiest, not that they are likely to have any of this particular material on hand.

Ken do you have a 1 gram piece for Dudley?

Folks, would we call this Chrome-Moly Steel, with alloy to be determined later?

Geo