Re: Trinitite
What is interesting is the ratio of intensity of 235/238. Of course, nuclide production, decay activity and contribution of Unat must be considered but it still seems
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WILLIAM S Dubyk
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#1246
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Re: Trinitite
He did weigh the sample Steve, but then he digested it in Hydrofluoric and Nitric acid. after drying he must have measured it again? Anyhow I don't know but would guess yes they can do that.
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GEOelectronics@...
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#1245
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Re: Trinitite
Is there any way to convert intensity to ppm or ppt?
Steve
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Sent: Tuesday, September 29, 2020 4:05 PM
To: [email protected] <[email protected]>
Subject: Re: [XRF]
By
WILLIAM S Dubyk
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#1244
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Re: Si pin xrf ..1st go
Possibly a mix up.
I did a fresh scan cos I din save the previous mca file
I thought I picked up the same one
I do have many apron samples
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taray singh <sukhjez@...>
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#1243
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Re: Trinitite
"Neptunium", a YouTuber did an ICPMS mass-spectrum? of Trinitite.
From the data presented on isotope ratios these are of most interest to us:
Analysis? ? ?Intensity
U-235? ? ? ? ?
By
GEOelectronics@...
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#1242
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Re: Trinitite
Geo,
I think you¡¯ve gone as far as you can without calculating a Pu concentration from the Am and determining the x-ray yields. The Pu derived U x-ray peaks of La1, Lb1, Lg1 and Ll you see in the
By
Dude
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#1241
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Trinitite Analysis: Uranium Decay Schemes
*U-238*
Let's walk through Uranium Radioactive Decay Schemes, one U isotope at a time to clarify the
reason we see certain peaks on spectroscopy scans.
We use the convention in this science
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GEOelectronics@...
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#1240
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Re: Si pin xrf ..1st go
Taray,
Is this a different apron? The accumulation times and dates are different and the spectra look different
Sent: Tuesday, September 29, 2020 4:22 AM
To: [email protected]
Subject: Re: [XRF] Si
By
Dude
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#1239
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Re: Trinitite
A closer look at a Gamma RaySpectrum scan of Red Trinitite? (see pics in first post of this thread).
The picture and .mca attached are of a previous (19FED2020) scan of Red Trinitite
In the photo
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GEOelectronics@...
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#1238
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Re: Si pin xrf ..1st go
Here is the x ray apron file.
Taray
By
taray singh <sukhjez@...>
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#1236
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Re: Si pin xrf ..1st go
Guys
Thanks for the tips
Geo and I had a running commentary setup
Next time mca files will follow
Yep
Rubbery feet is blocking heat loss
Just din strike me..
I have a rounded block of metal
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taray singh <sukhjez@...>
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#1235
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Re: Si pin xrf ..1st go
Geo,
It looked like a 1024 conversion gain. Most Si detectors will use 2048 even at the expense of counting time. Count time, FWHM, and noise can be traded off using peaking time¡its always
By
Dude
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#1234
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Re: Si pin xrf ..1st go
Good to know that Thanks Dud.Some mass spectrometer test of Trinitite et. al results are out there on the internet, will gather a few and see if they are showing parent, decay and fission products
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GEOelectronics@...
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#1233
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Re: Si pin xrf ..1st go
LOD depends on the element but in general the XRF limit of detection at best is 0.5 ppm and above, so for a ppb range element you¡¯ll need to do ICP/MS. That can also get stable element isotopic
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Dude
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#1232
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Re: Trinitite
By
GEOelectronics@...
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#1231
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Re: Trinitite
I loaded the ZIP file to the c: documents/raddecay folder and extracted it there. Then did a shortcut of the exe file to the desktop.
You should be able to select where to install when you extract
By
Dude
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#1230
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Re: Si pin xrf ..1st go
Dud, with the XRF gun, what is the likelihood of detecting a unique element in a large Trinitite sample, when the element dispersed and total weight is 1x10e-9 grams? Say the sample was 28 grams.
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GEOelectronics@...
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#1229
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Re: Si pin xrf ..1st go
The same scale expansion can be done selecting the Select View box on the tool bar. The cursor changes to a + and by holding the left mouse button you can select the range to expand. Click the < >
By
Dude
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#1228
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Re: Si pin xrf ..1st go
Dude, I did the energy cal here when I built it. Used test sources.
Geo
To: [email protected]
Sent: Monday, September 28, 2020 12:42:20 PM
Subject: Re: [XRF] Si pin xrf ..1st go
Nice clean
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GEOelectronics@...
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#1227
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Re: Si pin xrf ..1st go
Nice clean spectra, lookin¡¯ good.
You can take the conversion gain up to 2048 channels which will get a bit more resolution at the expense of a longer count time.
If you are talking about a peak
By
Dude
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#1226
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