Thanks for the links The
Open Raman is the best technical DIY one I¡¯ve been following but he uses rather
expensive open beam Thorlabs parts ($3,000) where I want to use fiber. ?http://www.thepulsar.be/article/openraman-starter-edition/
I have a B&W 473nm Raman
laser and spectrometer but no software and for mineral work it¡¯ll have a lot of
fluorescence.
I run Ocean Optics and
Stellarnet spectrometers with both their factory software and Spectragryph for
optical reflectance and LIBS and Spectragryph for XRF and gamma spec. I was
planning on using one of those for the Raman but finding a single mode laser
cheap enough is a problem not to mention the dichroic and edge filter. However it
is in the bucket list.
RE: Raman spectroscopy - Certainly, I'll post something in it's own thread when
I get everything working. ?
In the meantime, here are a few things I've found:
Typically Raman and cheap do not go together -
much to my chagrin
I got started by looking at this project:?
I have also followed this project quite a
bit:?
He has a blog that gives more detail, especially
on his attempts to get a working CCD:?
I originally wanted to try to build the whole
thing from scratch - then I got impatient and realized I was going to need
a metal mill and/or drill press if I was going to fabricate everything
including the kinematic mounts - so instead I decided to modify an
existing microscope and hack together a makeshift spectrometer from Ocean
Optics surplus parts
Ocean Optics seem to be the Amptek of the
UV-VIS-NIR world and their products are widely supported by 3rd party
software, such as Spectagryph, which is appealing:
Probably the best implementation out there is the
Open Raman Project
The key (read: expensive) parts are:
Good dichroic mirror and band-block filter -
There used to be an Ebay store that sold a ton of surplus filters
(production overruns) from Omega Filters ()
but it looks like Omega was just acquired and the eBay store doesn't have
the thousands of filters that were there just a few months ago
Powerful, Monochromatic Laser - I use a lower
end JDS Uniphase laser, but it's a bit weak. Their higher end Coherent
Compass laser are more powerful with a more monochromatic beam - but not
cheap
Osram seems to be producing green LEDs that are
single mode and display a very monochromatic beam and they are cheap.
But, they typically come in at 510 or 520nm, whereas the traditional
lasers were 532nm because they were frequency doubled 1064nm IR lasers.
A lot of surplus optics out there are catered to the 532nm laser - e.g.
540nm cut off, which you wouldn't want for a 510nm laser
The problems I have had are:
properly launching the Raman output from the
microscope into a fiber - I just got some fiber collimators that I'll
experiment with
too much noise in the spectrometer at long integration
times - this means that I either need a more powerful laser or TEC
cooling of the CCD sensor or both
Thunder Optics is one of the cheaper turnkey
solutions but they are still not cheap
My favorite YouTube channel "Applied
Science" did an episode on a quick down and dirty Raman system that
shows cheap proof of concept:?