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Re: vacuum wax help?


 

I got nothing on the wax Dave, but it is good to hear chatter on the list.? My guess is that the water was in the oil of the vacuum pump.? Vacuum oil is cheap so change it out often.? I am cheap too so I let my old oil sit in a plastic?container for a year or two and then pour off the clean stuff that is floating above the sludge.? the oil itself never really wears out.??

I would be amazed if that wax was really the seal for a vacuum system.? have you removed it and looked to see if them wires actually?attach to something that has a gasket.? copper gaskets never age out but people use buna or viton sometimes and that does have a shelf life.? Look for stuff like that.? The wax may just be some high voltage silicone putty sitting over the high vacuum electrical passthru pins.??

Dont SEM's have scintillation crystals or something that die if they sit in air for too long.? I not up on SEM's but interested in your rebuild.??

Oh,? I have a 68" dia x 68" deep vacuum chamber free to a good home for a tax write off letter if anybody knows a school looking for a great Mars simulation chamber.? contact me directly if you think this is your next great adventure.??

Drew in sunny Florida?

On Sun, Apr 3, 2022 at 6:07 PM Dave McGuire <mcguire@...> wrote:

? ?Hey folks, this list sure has been quiet lately.

? ?I'm restoring an Amray 1200 bench-top SEM, and my attention has
turned to the vacuum system.? The instrument has been down to air and
stored in a garage for 20+ years.

? ?I have some experience with vacuum, but not much.

? ?With all of the valves closed, pumping with a rotary pump against
about half a meter of the internal plumbing, I can get down to about 20
millitorr repeatably, if the TC gauge is to be believed.? It took about
a day to reach that point, but now I can get there from atmospheric
pressure in a minute or so.? I presume that was adsorbed water.

? ?Now I'm opening the roughing valve and trying to pump down the column
and chamber.? This significantly increases the volume of the system
that's being pumped, so I'm expecting days of getting rid of the water.
But, leaving it running overnight last night, it didn't budge from ~220
millitorr.? I assume there's a leak.

? ?Hunting around with my cheap-but-functional ultrasonic leak detector,
I've found that there's a big ugly wax seal at the top of the column
where the filament and HV leads enter the electron gun assembly.? See
attached photo. (if this mailing list is set up to allow such
attachments)? There's a significant leak right there, which changes as I
massage that gloopy waxy stuff around.

? ?I think that wax may have deteriorated with age.? It's pliable, but
it doesn't seem to adhere very well to anything, including the wires
it's supposed to create a seal around.

? ?Does anyone know what this stuff is, where I can get more (that I can
afford), or in general have any other thoughts or advice about this?

? ?This is a stately instrument that's in really good shape, all things
considered, and I'd love to get it running again.

? ? ? ? ? ? ?Thanks,
? ? ? ? ? ? ?-Dave

--
Dave McGuire, AK4HZ
New Kensington, PA





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