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Mini X-ray xrf
taray singh
Hi guys This is??my X-ray setup My x ray generating tube sits within a cylindrical??X-ray??collimator? This collimator protrudes into??a cardboard box??containing my X-ray detector??and X-ray signal detecting Inspector Usb Geiger counter. The exit of the X-ray collimator is closed by a less than 0.5 mm Al sheet? The back is a leaded glass with lead polymer sleeves ..to prevent backscatter from the rear and of my collimator? My X-ray generating tube is placed in such a way that the cathode is closest to the exit of X-ray beam? Applying the anode heel effect. I chose a low Z element Cr about 4 by 2 cm approx??for xrf and titanium orthopedic implant. Since my tube is not an x -ray tube ,it will not tolerate continuous firing? So I did it with intermittent shots each lasting about 1 sec Probably a 70 kvp will be more damaging than a 30 kvp like in my setup You notice a polymer covering for almost everything? This is a probably antimony polymer from some old stripped medical X-ray aprons courtesy of??a hospital where I work.The X-ray glass was also surplus from my hospital . Should be sufficient to block 30 kvp X-ray? Using multiple layers of apron material just in case. Pics are for my setup,transformer and an exact replica of my X-ray collimator??and a??Cr and Ti pic Apologies for not showing the X-ray generating tube. Taray ![]()
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It looks good Taray, one thing to try, repeat the setup but put the sample away from the source, sort of like a mirror that the source and sensor are both looking at the same surface? Geo ----- Original Message ----- From: taray singh via Groups.Io <sukhjez@...> To: [email protected] Sent: Fri, 21 Feb 2020 23:02:22 -0500 (EST) Subject: [XRF] Mini X-ray xrf Hi guys This is??my X-ray setup My x ray generating tube sits within a cylindrical??X-ray??collimator? This collimator protrudes into??a cardboard box??containing my X-ray detector??and X-ray signal detecting Inspector Usb Geiger counter. The exit of the X-ray collimator is closed by a less than 0.5 mm Al sheet? The back is a leaded glass with lead polymer sleeves ..to prevent backscatter from the rear and of my collimator? My X-ray generating tube is placed in such a way that the cathode is closest to the exit of X-ray beam? Applying the anode heel effect. I chose a low Z element Cr about 4 by 2 cm approx??for xrf and titanium orthopedic implant. Since my tube is not an x -ray tube ,it will not tolerate continuous firing? So I did it with intermittent shots each lasting about 1 sec Probably a 70 kvp will be more damaging than a 30 kvp like in my setup You notice a polymer covering for almost everything? This is a probably antimony polymer from some old stripped medical X-ray aprons courtesy of??a hospital where I work.The X-ray glass was also surplus from my hospital . Should be sufficient to block 30 kvp X-ray? Using multiple layers of apron material just in case. Pics are for my setup,transformer and an exact replica of my X-ray collimator??and a??Cr and Ti pic Apologies for not showing the X-ray generating tube. Taray |
taray singh
¿ªÔÆÌåÓýGeoThis involves moving the detector ?slightly away from the sample ?and realigning the specimen at an angle such that the incoming beam and detector are looking at the same sample ?broad surface.This will increase the surface area of excitement? Only drawback is longer distance ?sample to detector? I was placing more emphasis on distance and sacrificing surface area of contact? I hope this is what you meant . I will give it a shot ?next time? Taray On 22 Feb 2020, at 11:34 PM, GEOelectronics@... wrote:
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Yes that is what I mean. Mine is set op so rays are at 90 degrees to detector, the samples is in the rays but set at 45 degrees so the new rays go to the detector. our yield should increase many times since the new rays come from the excited surface. Geo ----- Original Message ----- From: taray singh via Groups.Io <sukhjez@...> To: [email protected] Sent: Sat, 22 Feb 2020 11:12:55 -0500 (EST) Subject: Re: [XRF] Mini X-ray xrf Geo This involves moving the detector ?slightly away from the sample ?and realigning the specimen at an angle such that the incoming beam and detector are looking at the same sample ?broad surface.This will increase the surface area of excitement? Only drawback is longer distance ?sample to detector? I was placing more emphasis on distance and sacrificing surface area of contact? I hope this is what you meant . I will give it a shot ?next time? Taray On 22 Feb 2020, at 11:34 PM, GEOelectronics@... wrote:
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Nice work and great re-use of available materials.? On Fri, Feb 21, 2020, 10:02 PM taray singh via Groups.Io <sukhjez=[email protected]> wrote:
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