Here's some info on loss tangent from David W. Knight, G3YNH, site
He mentions the microwave heating test is invalid because the properties of a material at microwave frequencies may be very different than at HF. Here's a clip of the info he provides on loss tangent by material type. Since I have some blue PEX tubing, which is cross-linked polyethylene and PE is listed as excellent,? I thought of making a trial toroid from 1/2 inch PEX. It's 22mm x 10mm x 10 mm (7/8" x 3/8" x 3/8") in size. Low res photo attached. It may be easier to stuff a 1/2" piece inside a 3/4" or 1" piece of PEX to increase the wall thickness.